Studies on the identification of psychotropic substances. VI. Preparation and various analytical data of reference standards of some hallucinogens, 2,5-dimethoxy-4-methylamphetamine (STP) , 2,5-dimethoxy-4-bromoamphetamine (DOB) and 2,5-dimethoxy-4-ethylamphetamine (DOET)
Shimamine, M.; Takahashi, K.; Nakahara, Y.
Eisei Shikenjo Hokoku. Bulletin of National Institute of Hygienic Sciences 1989(107): 113-119
1989
ISSN/ISBN: 0077-4715 PMID: 2636911 Document Number: 759
The Reference Standards of 2,5-dimethoxy-4-methylamphetamine (STP), 2,5-dimethoxy-4-bromoamphetamine (DOB) and 2,5-dimethoxy-4-ethylamphetamine (DOET) were prepared. Their purities measured by HPLC were 99.5% for STP hydrochlorie, 99.8% for DOB hydrobromide and 99.5% for DOET hydrochloride. For the identification and determination, various analytical data of the three drugs were obtained by using UV, IR, HPLC, GC/MS and NMR, and the discrimination were discussed.
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