A new stilbene glycoside from Dryopteris sublaeta
Feng, W.-s.; Cao, X.-w.; Kuang, H.-x.; Zheng, X.-k.
Yao Xue Xue Bao 40(12): 1131-1134
2005
ISSN/ISBN: 0513-4870 PMID: 16496679 Document Number: 587561
To study the chemical constituents of Dryopteris sublaeta Ching et Hsu. Fresh plant of Dryopteris sublaeta ching et hsu was extracted twice with boiling water, concentrated to small volume under reduced pressure at 50 degrees C. The concentrated material was partitioned with ether, ethyl acetate, and n-butanol. The fraction of ethyl acetate extract was chromatographed over macroporous adsorption resin (Diaion HP-20) eluted with a mixture of H2O and MeOH in increasing MeOH content. Their fractions from resin were repeatedly chromatographed over Toyopearl HW-40, Sephadex LH-20 and silica gel column chromatography. The compounds were identified on the basis of their physiochemical and spectral data. Four compounds were obtained and identified as 3,5-dihydroxy-stilbene-3-O-neohesperidoside (1), 3,5-dihydroxy-stilbene-3-O-beta-D-glucoside (2), polydotin peceid (3) and 3,5,4'-trihydroxy-bibenzyl-3-O-beta-D-glucoside (4). Compound 1 is a new compound, the others were isolated from Dryopteris for the first time.