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Studies on the lignan chemical constituents from pine needles of Pinus massoniana Lamb

Feng, W-sheng.; Bi, Y-feng.; Zheng, X-ke.; Wang, X-liang.; Li, J.

Yao Xue Xue Bao 38(3): 199-202

2003

ISSN/ISBN: 0513-4870
PMID: 12830716
Document Number: 558447
Various chromatographic techniques were used to separate and purify the chemical constituents of Pinus massoniana needles. The physicochemical properties and spectral data were used to elucidate the structures. Three compounds were isolated from the n-BuOH fraction of water extracts. The structures were identified as (7S,8R)-4,9'-dihydroxyl-3, 3'-dimethyoxyl-7, 8-dihydrobenzofunan-1'-propanolneolignan-9-O- alpha -L-rham nopyranoside (massonianoside D, 7), 4,4',9,9'-tetrahydroxyl-3,3'-dimethyoxyl-tetrahydrocyclolignan ((+)-isolariciresinol, 8) and 4,4',9'-trihydroxyl-3,3'-dimethyoxyl-tetrahydrocyclolignan-9-O- beta Dxylopyranoside (isolariciresinol-9-O-xyloside, 9). Compound 7 is a new compound, while compounds 8 and 0 9 were isolated from this plant for the first time.

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