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Digitoxin Reference Standard (Control 951) of the National Institute of Health Sciences

Kitajima, A.; Maekawa, K.; Yoshii, K.; Komatsu, H.; Tanimoto, T.; Okada, S.

Eisei Shikenjo hokoku. Bulletin of National Institute of Hygienic Sciences 1996(114): 113-115

1996

ISSN/ISBN: 0077-4715
PMID: 9037877
Document Number: 455496
The raw material of digitoxin was tested for preparation of the "Digitoxin Reference Standard (Control 951)". Analytical data obtained were as follows: loss on drying, 0.0%; infrared spectrum, the same as that of the JP Digitoxin Reference Standard (Control 845); thin-layer chromatography, no impurity was detected; high-performance liquid chromatography (HPLC), two kinds of impurities were detected and the total amount was estimated to be 0.16 +/- 0.01% (n = 3); assay, 99.0% by HPLC. Based on the above results, the raw material was authorized as the JP Digitoxin Reference Standard (Control 951).

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