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Ergocalciferol Reference Standard (Control 871) of National Institute of Hygienic Sciences

Tanaka, M.; Hiroshige, R.; Murai, M.; Tokunaga, H.; Okada, S.; Kimura, T.

Eisei Shikenjo hokoku. Bulletin of National Institute of Hygienic Sciences 1989(107): 151-153

1989

ISSN/ISBN: 0077-4715
PMID: 2636921
Document Number: 332091
The Ergocalciferol Reference Standard (Control 871) for the Japanese Pharmacopoeia was prepared. The following analytical data were obtained: melting point, 115.9 degrees C; infrared spectrum, same as the Japanese Pharmacopoeia Standard "Ergocalciferol Standard (Control 851)"; absorbance, E1%1cm (265 nm) = 464.8; optical rotation, ɑ20D = +104.7 degrees; thin-layer chromatography, same as the Japanese Pharmacopoeia Standard; high-performance liquid chromatography, contaminants were not detected; assay, 101.2%. On the basis of those results, this material was authorized as the Japanese Pharmacopoeia Standard (control 871).

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