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Preparation and characteristics of new coating for solid-phase microextraction

Yang, M.; Wang, Y.-l.; Zeng, Z.-r.; Zhou, Y.

Se Pu 20(3): 202-206

2002

ISSN/ISBN: 1000-8713
PMID: 12541936
Document Number: 544477
Poly (methylphenylvinylsiloxane) (PMPVS) coating for solid-phase microextraction (SPME) was first prepared by using sol-gel approach and cross-linking of free radical initiation. The extraction properties of the novel coating for aromatic compounds were investigated using a self-made SPME device coupled with a gas chromatograph-flame ionization detector (GC-FID). The coating provided high surface areas and allowed high extraction efficiency. Compared with some commercial SPME stationary phases, the new phase showed better selectivity and sensitivity toward aromatic compounds. Furthermore, PMPVS coating showed good thermal stability and longer lifetime.

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Pluscec, J.; Owies, S. 1987: Determination of vitamin D3 in liquid multivitamin preparation, using reverse phase, solid phase extraction liquid chromatography Journal - Association of Official Analytical Chemists 70(3): 599-601
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Litvinovich, N.E.; Nosik, D.N.; Novokhatskiĭ, A.S. 1986: Optimization of conditions for preparation of the solid phase of infected cells in the immunoenzyme analysis of monoclonal antibodies Molekuliarnaia Genetika Mikrobiologiia i Virusologiia 5: 39-44
Sugiura, M.; Mizuoka, K. 1995: Kinds and characteristics of solid-phase enzyme immunoassay Nihon Rinsho. Japanese Journal of Clinical Medicine 53(9): 2188-2191
Naruto, M. 1982: Synthesis of oligodeoxyribonucleotides by solid phase phosphotriester method on a reduced scale; preparation of oligonucleotides for improved promoter sequence Nucleic Acids Symposium Series 11: 77-80