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Partition chromatography of barbiturates in combinations with salicylamide and other drugs

Hall, R.J.; Levine, J.

Journal - Association of Official Analytical Chemists 55(2): 332-334

1972

ISSN/ISBN: 0004-5756
PMID: 4666193
Document Number: 45909
Barbiturates can be separated from salicylamide by trapping the latter on a partition chromatographic column in which ferric chloride or ferric chloride-urea is the immobile phase, and isooctane-ether mixtures are the mobile phase. Experimental conditions must be selected in accord with the partition characteristics of the individual barbiturate. Analyses are presented of commercial preparations of amobarbital, pentobarbital, and butabarbital with salicylamide together with a variety of other drugs.

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Gerasimova, T.I.; Buniatian, A.F.; Volchek, A.G. 1979: Use of column chromatography to partition combinations of steroid hormones and quantitative determination by saturation analysis (review of the literature) Laboratornoe Delo 1979(2): 67-74
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Xu, X.R.; Xu, H.; Lu, Y.A.; Ghen, J. 1979: Determination of partition coefficient by high-pressure liquid chromatography. I. Determination of partition coefficient of cinnamic acids and related compounds by reversed-phase high-pressure liquid chromatography Yao Xue Xue Bao 14(4): 246-252
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Crommen, J. 1977: Separation and individual determination of four sulfonamides in mixture by column partition chromatography Journal de Pharmacie de Belgique 32(2): 128-142
Brown, P.R.; Krstulović, A.M.; Hartwick, R.A. 1977: Analysis of purines and their nucleosides by the reverse phase partition mode of high pressure liquid chromatography Advances in Experimental Medicine and Biology 76a: 610-618
Lis, A.W.; Hayes, S.J. 1972: Studies on 5-hydroxyuridine (isobarbituridine): VIII. Instability in partition chromatography solvent ethylacetate-1-butanol-ligroin-water Physiological Chemistry and Physics 4(4): 377-386
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Tassinari, C.A.; Roger, J. 1975: Prognosis and therapy of complex partial seizures with barbiturates, hydantoins, and other drugs Advances in Neurology 11: 201-219
Brånstad, J.O.; Meresaar, U.; Agren, A. 1972: Complex formation between macromolecules and drugs. VII. the binding of some barbiturates to human serum albumin (HSA) at varying pH Acta Pharmaceutica Suecica 9(2): 129-134
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Liu, Z.; Li, Y.; Jiang, S.; Chen, L. 1997: The combinations of separation modes in multidimensional high performance liquid chromatography (MDHPLC) Se Pu 15(6): 490-493
Getova, D.; Georgiev, V. 1987: GABA-ergic mechanisms in the anticonvulsive activity of newly-synthesized barbiturates. I. Effects of barbiturates on the convulsive action of GABA-antagonists Acta Physiologica et Pharmacologica Bulgarica 13(3): 43-50
Maresova, V.; Chadt, J.; Novakova, E. 2008: Screening and semiquantitative analysis of drugs and drugs of abuse in human serum samples using gas chromatography-mass spectrometry Neuro Endocrinology Letters 29(5): 749-754
Matsumoto, K.; Kikuchi, H.; Kano, S.; Iri, H.; Takahashi, H.; Umino, M. 1988: Automated determination of drugs in serum by liquid chromatography with column-switching. I. Separation of antiepileptic drugs and metabolites Clinical Chemistry 34(1): 141-144
Moffat, A.C.; Stead, A.H.; Smalldon, K.W. 1974: Optimum use of paper, thin-layer and gas-liquid chromatography for the identification of basic drugs. 3. Gas-liquid chromatography Journal of Chromatography 90(1): 19-33
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Schuh, F.T. 1981: On the interaction of combinations of nondepolarizing neuromuscular blocking drugs Der Anaesthesist 30(11): 537-542
Domínguez de Villota, E.; Shubin, H.; Liu, V.Y.; Weil, M.H. 1983: Severe poisoning with barbiturates, glutethimide and other sedative drugs. (I) Clinical aspects, mortality and therapeutic aspects of 68 patients Revista Clinica Espanola 171(6): 409-413
Schawrz, M.A.; Raith, K.; Dongowski, G.; Neubert, R.H. 1998: Effect on the partition equilibrium of various drugs by the formation of mixed bile salt/phosphatidylcholine/fatty acid micelles. A characterization by micellar affinity capillary electrophoresis. Part IV Journal of Chromatography A 809(1-2): 219-229