Chelate extraction and flame atomic absorption spectrometric determination of nanogram amounts of manganese in blood and animal tissue
Shearer, D.A.; Cloutier, R.O.; Hidiroglou, M.
Journal - Association of Official Analytical Chemists 60(1): 155-159
1977
ISSN/ISBN: 0004-5756 PMID: 188801 Document Number: 111209
The sample is digested with HClO4 and HNO3 and Mn complexed with sodium diethyldithiocarbamate is extracted with methyl isobutyl ketone and estimated by spectrometry. The limit of detection is about 10 ng Mn/ml of aspirate, 0.05 N HCl in acetone and water (9:1), or 2 ng/ml of bovine blood for a 20-ml sample.
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