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Study on separation and purification of anthraquinones in radix et rhizoma rhei by D301 macroporous resin

Xu, H.-L.; Chen, J.; Shao, J.-Z.; Sun, Y.; Zhang, C.-Z.

Zhongguo Zhong Yao Za Zhi 31(14): 1163-1165

2006

ISSN/ISBN: 1001-5302
PMID: 17048585
Document Number: 597220
The parameters of absorption and purification of total anthraquinones in Radix Et Rhizoma Rhei by D301 macroporous resin were investigated in this paper. HPLC was used to analyze the content of total anthraquinones in Radix Et Rhizoma with emodin as control. The appropriate adsorption conditions were: concentration of extract 0.5 g x mL(-1); pH 9; flow rate 1 BV x h(-1). When the 75% ethanol was used as elution and the concentration of HCl was 0.1 mol x L(-1), and the flow rate was 1.0 BV x h(-1), the effect of desorption was satisfactory. D301 resin provided a good effect on the exchang and absorption of total anthraquinones in Radix Et Rhizoma.

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