Study on the analytical method of s-triazine herbicide residues in soil and maize
Liu, F.; Mu, W.; Wang, J.; Yu, J.
Se Pu 16(6): 543-544
1998
ISSN/ISBN: 1000-8713 PMID: 11938923 Document Number: 494264
The sample was extracted with a mixture of V(acetonitrile): V(methanol) = 1:1. After filtration, the extract was defatted with petroleum ether and then it was passed through a short C18 column for pretreatment and analysed by Nova-Pak C18 column, 150 mm x 3.9 mm i.d., with V(MeOH): V(H2O) = 55:45 as mobile phase. The recoveries were 82.4%-99.8% for cyanazine, 85.6%-102.3% for atrazine and 89.1%-108.4% for simetryne.
Document emailed within 1 workday
Related Documents
Otsuki, K.; Sekita, H.; Takeda, Y.; Ito, Y.; Takeda, M. 1971: Studies on the analysis of pesticide residues in foods. IV. Analytical method of organo-chlorinated pesticides residues in agricultural products Eisei Shikenjo Hokoku. Bulletin of National Institute of Hygienic Sciences 89: 38-43Năstasă, V.; Cuciureanu, R. 1984: Analytical study of triazine herbicides Revista Medico-Chirurgicala a Societatii de Medici Si Naturalisti Din Iasi 88(2): 319-323
Wang, X.-C.; Yang, W.-Y.; Deng, X.-Y.; Zhang, Q.; Yong, T.-W.; Liu, W.-G.; Yang, F.; Mao, S.-M. 2014: Effects of nitrogen management on maize nitrogen utilization and residual nitrate nitrogen in soil under maize/soybean and maize/sweet potato relay strip intercropping systems Ying Yong Sheng Tai Xue Bao 25(10): 2868-2878
Sekita, H.; Sasaki, K.; Kawamura, Y.; Takeda, M.; Uchiyama, M. 1982: Studies on analysis of pesticide residues in foods (XXXVIII). Surveillance of chlorinated phenoxy herbicide residues in imported agricultural crops in 1980 Eisei Shikenjo Hokoku. Bulletin of National Institute of Hygienic Sciences 100: 193-194
Teranishi, Y.; Takeda, M.; Uchiyama, M. 1975: Studies on the analysis of pesticide residues in food. (XVII). Analytical method of tetrachloroisophthalonitrile residue in agricultural products Eisei Shikenjo Hokoku. Bulletin of National Institute of Hygienic Sciences 93: 41-45
Li, Z-xin.; Dong, S-ting.; Wang, K-jun.; Liu, P.; Zhang, J-wang.; Wang, Q-cheng.; Liu, C-xiao. 2008: Soil nutrient leaching patterns in maize field under different fertilizations: an in situ study Ying Yong Sheng Tai Xue Bao 19(1): 65-70
Khan, S.U. 1975: Electron capture gas-liquid chromatographic method for the simultaneous analysis of 2,4-D, dicamba, and mecoprop residues in soil, wheat, and barley Journal - Association of Official Analytical Chemists 58(5): 1027-1031
el-Dahtory, T.A.; Stenz, E.; Schuster, G. 1984: Degradation and utilization of 2,4-dioxohexahydro-1,3,5-triazine (DHT) by soil microorganisms Zentralblatt für Mikrobiologie 139(5): 375-382
Lopatykhin, E.I.; Puzakov, S.A.; Popkov, V.A. 1989: Gas-chromatographic analysis of herbicide residues in medicinal raw materials Gigiena i Sanitariia 6: 47-49
Adler, I.L.; Gordon, C.F.; Haines, L.D.; Wargo, J.P. 1972: Determination of residues from herbicide N-(1,1-dimethylpropynyl)-3, 5-dichlorobenzamide by electron capture gas-liquid chromatography Journal - Association of Official Analytical Chemists 55(4): 802-805
Gordienko, N.I. 1977: Hygienic establishment of the maximum permissible concentration of the herbicide, prometryne, in soil Gigiena i Sanitariia 1: 22-25
Rouchaud, J.; Neus, O.; Eelen, H.; Bulcke, R. 2001: Dissipation and mobility of the sulfonylaminocarbonyl-triazolinone herbicide propoxycarbazone in the soil of winter wheat crops Mededelingen 66(2b): 713-721
Yang, L.; Cai, Z. 2005: Effects of N application and maize growth on N2O emission from soil Ying Yong Sheng Tai Xue Bao 16(1): 100-104
Jiang, Y.; Zhuang, Q.-L.; Zhang, Y.-G.; Liang, W.-J. 2008: Distribution characteristics of soil phosphorus in maize belt farmlands of Northeast China Ying Yong Sheng Tai Xue Bao 19(9): 1931-1936
Zhang, J.-E.; Gao, A.-X.; Xu, H.-Q.; Luo, M.-Z. 2009: Effects or maize/peanut intercropping on rhizosphere soil microbes and nutrient contents Ying Yong Sheng Tai Xue Bao 20(7): 1597-1602
Lentini, J.J. 2000: Analytical methods for ignitable liquid residues Journal of Forensic Sciences 45(6): 1358
Sannino, A. 1998: Determination of phenylurea herbicide residues in vegetables by liquid chromatography after gel permeation chromatography and Florisil cartridge cleanup Journal - Association of Official Analytical Chemists 81(5): 1048-1053
Cencelj, J.; Dorer, M. 1974: Pesticide residues in soil and water Arhiv Za Higijenu Rada i Toksikologiju 25(2): 253-256
Benoit, M.O.; Jaffray, P.; Caillens, H.; Souciet, C.; Ekindjian, O.G.; Douris, R.G. 1981: Serum isoamylases determination. Analytical and critical study of a new method using an inhibitor protein Pathologie-Biologie 29(4): 223-228
Zhao, Y.; Chen, J.; Wang, X. 1998: Study on the analytical method for organochlorine pesticide residue using gas chromatography-mass spectrometry Wei Sheng Yan Jiu 27(6): 425-428