Rapid determination of aflatoxin M1 in milk and dairy products by high-performance liquid chromatography
Chambon, P.; Dano, S.D.; Chambon, R.; Geahchan, A.
Journal of Chromatography 259(2): 372-374
1983
ISSN/ISBN: 0021-9673 PMID: 6406527 Document Number: 200284
A preliminary extraction using Zn(OH)2 precipitation is followed by hexane clean-up. Subsequently a vacuum concentrated chloroform extract is injected on to a C18 grafted silica column and eluted with acetonitrile:methanol:water (20:5:75). The method is accurate and reliable, giving a recovery of approx. 80% and, through an efficient clean-up of the milk sample, allows rapid determination of aflatoxin M1 with a detection limit of 10 ng/l milk.
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