Effect of ceramic surface treatment on the shear bond strength of a resin cement to different ceramic systems
Ribeiro, J.G.R.; Segalla, J.C.M.; Perez, F.; Ribeiro, J.C.R.; Moyses, M.R.
General Dentistry 60(5): E315-E320
2012
ISSN/ISBN: 0363-6771 PMID: 23032240 Document Number: 657710
This study evaluated three surface treatments and their effect on the shear bond strength between a resin cement and one of three ceramics. The ceramic surfaces were evaluated with scanning electron microscopy (SEM) as well. Specimens were treated with 50 μm aluminum oxide airborne particles, 10% hydrofluoric acid etching, or a combination of the two. Using a matrix with a center hole (5.0 mm x 3.0 mm), the ceramic bonding areas were filled with resin cement following treatment. The specimens were submitted to thermal cycling (1,000 cycles) and the shear bond strength was tested (0.5 mm/minute). The failure mode and the effect of surface treatment were analyzed under SEM. Data were submitted to ANOVA and a Tukey test (α = 0.05). Duceram Plus and IPS Empress 2 composite specimens produced similar shear bond strength results (p > 0.05), regardless of the treatment method used. Hydrofluoric acid decreased the shear bond strength of In-Ceram Alumina specimens. For all materials, surface treatments changed the morphological surface. All treatments influenced the shear bond strength and failure mode of the ceramic/resin cement composites.